Lab Manual: Refractive Index of Glass Slab

Determination of Refractive Index of a Glass Slab

1. Aim

To determine the refractive index of a glass slab using a travelling microscope.

2. Apparatus Used

  • Travelling microscope with vernier scale
  • Glass slab of uniform thickness
  • White paper with a fine ink mark
  • Spirit level
  • Laboratory stand with clamps
  • Clean piece of cloth
  • Micrometer screw gauge (for measuring thickness of the slab)

3. Diagram

Experimental setup showing a travelling microscope focused on a glass slab with marked positions for real and apparent positions of a mark

Fig.1: Experimental setup for determination of refractive index using a travelling microscope

4. Theory

When a ray of light passes from one medium to another, it bends or refracts according to Snell's law. The refractive index of a medium is defined as the ratio of the speed of light in vacuum to the speed of light in that medium.

In this experiment, we use a travelling microscope to measure the apparent shift in position of a mark when viewed through a glass slab. When we observe a mark through a glass slab, the mark appears to be raised due to refraction of light at the two parallel surfaces of the glass slab.

Consider a point object O placed below a glass slab of thickness t and refractive index μ. When viewed from above, the object appears to be at position I which is at a height t' from the bottom surface of the glass slab.

According to the laws of refraction:

$\mu = \frac{\sin i}{\sin r}$

For small angles of incidence and refraction, we can write:

$\mu = \frac{t}{t'}$

Where:

  • t = actual thickness of the glass slab
  • t' = apparent thickness of the glass slab

The apparent thickness (t') is less than the actual thickness (t) of the glass slab. By measuring both these quantities using a travelling microscope, we can determine the refractive index of the glass slab.

5. Formula

The refractive index of the glass slab is given by:

$\mu = \frac{\text{Real thickness of the glass slab}}{\text{Apparent thickness of the glass slab}} = \frac{t}{t'}$

Where:

  • Real thickness (t) = Direct measurement of thickness using micrometer screw gauge or difference of microscope readings when focused on top and bottom surfaces of the glass slab
  • Apparent thickness (t') = Difference between the microscope readings when focused on the mark directly and when focused on the mark through the glass slab

Alternative formula using the microscope readings:

$\mu = \frac{h_2 - h_1}{h_3 - h_2}$

Where:

  • h₁ = Reading when microscope is focused on the mark directly
  • h₂ = Reading when microscope is focused on the bottom surface of the glass slab
  • h₃ = Reading when microscope is focused on the top surface of the glass slab

6. Procedure

  1. Setup Preparation:
    • Place a sheet of white paper with a fine ink mark on the laboratory table.
    • Level the travelling microscope using the spirit level and adjusting screws.
    • Ensure the microscope tube can move smoothly in the vertical direction.
  2. Measurement of Direct Reading (h₁):
    • Focus the microscope on the ink mark on the paper.
    • Note the reading on the vertical scale of the microscope (h₁).
  3. Placement of Glass Slab:
    • Clean the glass slab with a soft cloth to remove any dust or fingerprints.
    • Place the glass slab carefully over the mark, ensuring the slab is perfectly horizontal.
  4. Measurement of Bottom Surface Reading (h₂):
    • Focus the microscope on the bottom surface of the glass slab.
    • Note the reading on the vertical scale (h₂).
  5. Measurement of Top Surface Reading (h₃):
    • Move the microscope upward and focus it on the top surface of the glass slab.
    • Note the reading on the vertical scale (h₃).
  6. Measurement of Mark Through Glass (h₄):
    • Without disturbing the glass slab, focus the microscope on the ink mark as seen through the glass slab.
    • Note the reading on the vertical scale (h₄).
  7. Measurement of Glass Thickness:
    • Calculate the real thickness of the glass slab: t = h₃ - h₂
    • Calculate the apparent thickness: t' = h₄ - h₂
  8. Repeat Measurements:
    • Repeat the above steps at least 5 times by focusing on different portions of the mark.
    • Record all readings in the observation table.

7. Observation Table

Least count of the travelling microscope = ________ mm

Thickness of glass slab measured by micrometer screw gauge = ________ mm

S.No. Reading when focused on the mark directly (h₁) Reading when focused on the bottom surface of glass slab (h₂) Reading when focused on the top surface of glass slab (h₃) Reading when focused on the mark through glass slab (h₄) Real thickness of glass slab (t = h₃ - h₂) mm Apparent thickness (t' = h₄ - h₂) mm Refractive index (μ = t/t')
1
2
3
4
5

8. Calculations

For each observation:

  1. Calculate the real thickness of the glass slab (t):

    t = h₃ - h₂

  2. Calculate the apparent thickness (t'):

    t' = h₄ - h₂

  3. Calculate the refractive index (μ):

    $\mu = \frac{t}{t'} = \frac{h_3 - h_2}{h_4 - h_2}$

Calculate the mean value of refractive index:

$\mu_{mean} = \frac{\mu_1 + \mu_2 + \mu_3 + \mu_4 + \mu_5}{5}$

9. Result

The refractive index of the given glass slab is μ = _________ (with appropriate significant figures)

Standard value of refractive index for glass = 1.5

Percentage error = $\frac{|\text{Experimental Value} - \text{Standard Value}|}{\text{Standard Value}} \times 100\%$ = __________%

10. Precautions

  1. The travelling microscope should be perfectly vertical and its movement should be smooth.
  2. The glass slab should be placed perfectly horizontal on the paper with mark.
  3. The glass slab should be clean and free from dust and fingerprints.
  4. The ink mark should be fine and clear.
  5. There should be proper illumination for clear focusing.
  6. Parallax error should be avoided while taking the readings.
  7. Focus the microscope carefully to get sharp images of the mark and the surfaces.
  8. Avoid touching the optical surfaces of the microscope lens.
  9. The reading should be taken without disturbing the setup.
  10. The microscope should be focused by moving it in one direction only to avoid backlash error.

11. Sources of Error

  1. Non-parallel faces of the glass slab can lead to distorted images.
  2. Imperfect focusing of the microscope can lead to incorrect reading.
  3. Presence of dust or fingerprints on the glass slab can affect the results.
  4. Non-uniform thickness of the glass slab can lead to variations in measurements.
  5. Improper leveling of the travelling microscope can cause systematic errors.
  6. Parallax errors while taking readings from the scale.
  7. Backlash error in the microscope movement.
  8. The mark might not be perfectly visible through the glass slab due to multiple reflections.
  9. Temperature variations can affect the refractive index of the glass.
  10. Human errors in reading the vernier scale.

12. Viva Voice Questions

Q1: What is refractive index?

A1: The refractive index of a medium is defined as the ratio of the speed of light in vacuum to the speed of light in that medium. Mathematically, μ = c/v, where c is the speed of light in vacuum and v is the speed of light in the medium.

Q2: State Snell's law of refraction.

A2: Snell's law states that the ratio of the sine of the angle of incidence to the sine of the angle of refraction is constant for a given pair of media. Mathematically, $\frac{\sin i}{\sin r} = \mu$, where μ is the refractive index of the second medium with respect to the first medium.

Q3: Why does an object appear raised when viewed through a glass slab?

A3: When light rays from an object pass through a glass slab, they bend away from the normal while exiting the slab (going from a denser to a rarer medium). This bending makes the light rays appear to come from a point that is closer to the surface than the actual object, making the object appear raised.

Q4: What is a travelling microscope and how does it work?

A4: A travelling microscope is a precision instrument used to measure small distances. It consists of a microscope mounted on a rigid frame with three mutually perpendicular scales (horizontal, vertical, and cross). The microscope can be moved along these scales, and the readings are noted using vernier scales for high precision.

Q5: How does the thickness of the glass slab affect the apparent position of the mark?

A5: The thicker the glass slab, the greater the apparent shift in position of the mark. The relationship between the real thickness (t) and apparent thickness (t') is given by t = μt', where μ is the refractive index of the glass.

Q6: What is the difference between real thickness and apparent thickness?

A6: The real thickness is the actual physical distance between the top and bottom surfaces of the glass slab. The apparent thickness is the perceived distance when looking through the glass slab due to refraction of light.

Q7: Why is the apparent thickness less than the real thickness?

A7: Due to refraction, light rays bend when they pass from one medium to another. This bending makes objects appear closer than they actually are when viewed through a denser medium like glass, causing the apparent thickness to be less than the real thickness.

Q8: What would happen to the refractive index if we use a liquid instead of a glass slab?

A8: The same principle applies to liquids. However, liquids typically have lower refractive indices than solids like glass. The experiment would be modified slightly to contain the liquid, but the formula μ = t/t' would still be valid.

Q9: How does the wavelength of light affect the refractive index?

A9: The refractive index of a material varies with the wavelength of light. This phenomenon is known as dispersion. Generally, shorter wavelengths (like blue light) have higher refractive indices than longer wavelengths (like red light) in transparent materials like glass.

Q10: What are the applications of knowing the refractive index of materials?

A10: Knowledge of refractive indices is important in designing optical instruments like microscopes, telescopes, cameras, and eyeglasses. It's also used in fiber optics, gemology for identifying precious stones, and in industries for quality control of materials.

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